Solving Problems with NMR Spectroscopy

Solving Problems with NMR Spectroscopy, Second Edition, is a fully updated and revised version of the best-selling book. This new edition still clearly presents the basic principles and applications of NMR spectroscopy with only as much math as is necessary. It shows how to solve chemical structures with NMR by giving many new, clear examples for readers to understand and try, with new solutions provided in the text. It also explains new developments and concepts in NMR spectroscopy, including sensitivity problems (hardware and software solutions) and an extension of the multidimensional coverage to 3D NMR. The book also includes a series of applications showing how NMR is used in real life to solve advanced problems beyond simple small-molecule chemical analysis. This new text enables organic chemistry students to choose the most appropriate NMR techniques to solve specific structures. The problems provided by the authors help readers understand the discussion more clearly and the solution and interpretation of spectra help readers become proficient in the application of important, modern 1D, 2D, and 3D NMR techniques to structural studies. Explains and presents the most important NMR techniques used for structural determinations Offers a unique problem-solving approach for readers to understand how to solve structure problems Uses questions and problems, including discussions of their solutions and interpretations, to help readers understand the fundamentals and applications of NMR Avoids use of extensive mathematical formulas and clearly explains how to implement NMR structure analysis Foreword by Nobel Prize winner Richard R. Ernst New to This Edition Key developments in the field of NMR spectroscopy since the First Edition in 1996 New chapter on sensitivity enhancement, a key driver of development in NMR spectroscopy New concepts such as Pulse Field Gradients, shaped pulses, and DOSY (Diffusion Order Spectroscopy) in relevant chapters More emphasis on practical aspects of NMR spectroscopy, such as the use of Shigemi tubes and various types of cryogenic probes Over 100 new problems and questions addressing the key concepts in NMR spectroscopy Improved figures and diagrams More than 180 example problems to solve, with detailed solutions provided at the end of each chapter

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  • Author : Atta-ur-Rahman
  • Publisher : Academic Press
  • Pages : 534 pages
  • ISBN : 0124116132
  • Rating : 4/5 from 21 reviews
CLICK HERE TO GET THIS BOOKSolving Problems with NMR Spectroscopy

Solving Problems with NMR Spectroscopy

Solving Problems with NMR Spectroscopy
  • Author : Atta-ur-Rahman,Muhammad Iqbal Choudhary,Atia-tul- Wahab
  • Publisher : Academic Press
  • Release : 18 August 2015
GET THIS BOOKSolving Problems with NMR Spectroscopy

Solving Problems with NMR Spectroscopy, Second Edition, is a fully updated and revised version of the best-selling book. This new edition still clearly presents the basic principles and applications of NMR spectroscopy with only as much math as is necessary. It shows how to solve chemical structures with NMR by giving many new, clear examples for readers to understand and try, with new solutions provided in the text. It also explains new developments and concepts in NMR spectroscopy, including sensitivity

Problems and Problem Solving in Chemistry Education

Problems and Problem Solving in Chemistry Education
  • Author : Georgios Tsaparlis
  • Publisher : Royal Society of Chemistry
  • Release : 17 May 2021
GET THIS BOOKProblems and Problem Solving in Chemistry Education

Problem solving is central to the teaching and learning of chemistry at secondary, tertiary and post-tertiary levels of education, opening to students and professional chemists alike a whole new world for analysing data, looking for patterns and making deductions. As an important higher-order thinking skill, problem solving also constitutes a major research field in science education. Relevant education research is an ongoing process, with recent developments occurring not only in the area of quantitative/computational problems, but also in qualitative

Essential Practical NMR for Organic Chemistry

Essential Practical NMR for Organic Chemistry
  • Author : S. A. Richards,J. C. Hollerton
  • Publisher : John Wiley & Sons
  • Release : 07 December 2010
GET THIS BOOKEssential Practical NMR for Organic Chemistry

This book describes the use of NMR spectroscopy for dealing with problems of small organic molecule structural elucidation. It features a significant amount of vital chemical shift and coupling information but more importantly, it presents sound principles for the selection of the techniques relevant to the solving of particular types of problem, whilst stressing the importance of extracting the maximum available information from the simple 1-D proton experiment and of using this to plan subsequent experiments. Proton NMR is covered

Organic Structures from Spectra

Organic Structures from Spectra
  • Author : L. D. Field,S. Sternhell,J. R. Kalman
  • Publisher : John Wiley & Sons
  • Release : 18 February 2013
GET THIS BOOKOrganic Structures from Spectra

The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. A critical part of any such course is a suitable set of problems to develop the student’s understanding of how structures are determined from spectra. Organic Structures from Spectra, Fifth Edition is a carefully chosen set of more than 280 structural problems employing the major modern spectroscopic techniques, a selection of 27 problems using 2D-NMR spectroscopy, more than 20 problems specifically dealing

Organic Structures from Spectra

Organic Structures from Spectra
  • Author : L. D. Field,S. Sternhell,John R. Kalman
  • Publisher : John Wiley & Sons Incorporated
  • Release : 26 December 1995
GET THIS BOOKOrganic Structures from Spectra

Offers a realistic approach to solving problems used by organic chemists. Covering all the major spectroscopic techniques, it provides a graded set of problems that develop and consolidate students' understanding of organic spectroscopy. This edition contains more elementary problems and a modern approach to NMR spectra.

One and Two Dimensional NMR Spectroscopy

One and Two Dimensional NMR Spectroscopy
  • Author : Atta-ur- Rahman
  • Publisher : Elsevier
  • Release : 22 October 2013
GET THIS BOOKOne and Two Dimensional NMR Spectroscopy

The field of nuclear magnetic resonance spectroscopy has undergone explosive development during the last decade with the advent of new one- and two-dimensional techniques. The author has had extensive experience in the use of these techniques for the structure elucidation of complex natural products, and in this book he gives a comprehensive, up-to-date and very readable account of these developments. The book's scope is very wide. It starts from fundamental principles of modern NMR spectroscopy, describing the instrumentation and its

Problems in Organic Structure Determination

Problems in Organic Structure Determination
  • Author : Roger G. Linington,Philip G. Williams,John B. MacMillan
  • Publisher : CRC Press
  • Release : 14 October 2015
GET THIS BOOKProblems in Organic Structure Determination

At a point where most introductory organic chemistry texts end, this problems-based workbook picks up the thread to lead students through a graduated set of 120 problems. With extensive detailed spectral data, it contains a variety of problems designed by renowned authors to develop proficiency in organic structure determination. This workbook leads you from basic problems encountered in introductory organic chemistry textbooks to highly complex natural product-based problems. It presents a concept-based learning platform, introducing key concepts sequentially and reinforcing them

Diffusion and Electrophoretic NMR

Diffusion and Electrophoretic NMR
  • Author : Peter Stilbs
  • Publisher : Walter de Gruyter GmbH & Co KG
  • Release : 19 August 2019
GET THIS BOOKDiffusion and Electrophoretic NMR

Diffusion and Eletrophoretic NMR experiments resolve chemical compounds based on their molecular motion. This publication introduces the basics of these methods and explains how they can be used to measure the size of molecules and aggregates, to determine degree of polymerization and to solve other chemical problems. Supplied with many case studies, the book is a must-have for students and researchers who work with practical NMR measurements.

Organic Structure Determination Using 2-D NMR Spectroscopy

Organic Structure Determination Using 2-D NMR Spectroscopy
  • Author : Jeffrey H. Simpson
  • Publisher : Academic Press
  • Release : 01 July 2022
GET THIS BOOKOrganic Structure Determination Using 2-D NMR Spectroscopy

"The second edition of this book comes with a number of new figures, passages, and problems. Increasing the number of figures from 290 to 448 has necessarily added considerable length, weight, and, expense. It is my hope that the book has not lost any of its readability and accessibility. I firmly believe that most of the concepts needed to learn organic structure determination using nuclear magnetic resonance spectroscopy do not require an extensive mathematical background. It is my hope that the manner

Assigning Inorganic NMR Spectra

Assigning Inorganic NMR Spectra
  • Author : Michael O'Neill
  • Publisher : Unknown Publisher
  • Release : 23 October 2019
GET THIS BOOKAssigning Inorganic NMR Spectra

Teach yourself how to assign the complex NMR spectra of main group molecules.This book offers advanced chemistry students the opportunity to engage deeply with the skill of assigning inorganic NMR spectra. Beginning simply, the book challenges you with a sequence of problems on environments, quadrupolar splitting, and spin dilution. Using worked answers, you self-mark your own answers to gain all the skills you need.Short interludes teach Hz-ppm conversions, the use of decoupling, molecular fluxionality, and how to calculate

Structural Biology

Structural Biology
  • Author : Quincy Teng
  • Publisher : Springer Science & Business Media
  • Release : 02 August 2007
GET THIS BOOKStructural Biology

Over the years since NMR was first applied to solve problems in structural biology, it has undergonedramaticdevelopmentsinbothNMRinstrumenthardwareandmethodology. While it is established that NMR is one of the most powerful tools for understanding biological p- cesses at the atomic level, it has become increasingly difficult for authors and instructors to make valid decisions concerning the content and level for a graduate course of NMR in str- turalbiology. BecausemanyofthedetailsinpracticalNMRarenotdocumentedsystematically, students entering the field have to learn the experiments and methods through communication

Experimental Approaches of NMR Spectroscopy

Experimental Approaches of NMR Spectroscopy
  • Author : The Nuclear Magnetic Resonance Society of Japan
  • Publisher : Springer
  • Release : 23 November 2017
GET THIS BOOKExperimental Approaches of NMR Spectroscopy

This book describes the advanced developments in methodology and applications of NMR spectroscopy to life science and materials science. Experts who are leaders in the development of new methods and applications of life and material sciences have contributed an exciting range of topics that cover recent advances in structural determination of biological and material molecules, dynamic aspects of biological and material molecules, and development of novel NMR techniques, including resolution and sensitivity enhancement. First, this book particularly emphasizes the experimental

Organic Structures from 2D NMR Spectra

Organic Structures from 2D NMR Spectra
  • Author : L. D. Field,H. L. Li,A. M. Magill
  • Publisher : John Wiley & Sons
  • Release : 30 March 2015
GET THIS BOOKOrganic Structures from 2D NMR Spectra

The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. Over recent years, a number of powerful two-dimensional NMR techniques (e.g. HSQC, HMBC, TOCSY, COSY and NOESY) have been developed and these have vastly expanded the amount of structural information that can be obtained by NMR spectroscopy. Improvements in NMR instrumentation now mean that 2D NMR spectra are routinely (and sometimes automatically) acquired during the identification and characterisation of

Understanding NMR Spectroscopy

Understanding NMR Spectroscopy
  • Author : James Keeler
  • Publisher : John Wiley & Sons
  • Release : 19 September 2011
GET THIS BOOKUnderstanding NMR Spectroscopy

This text is aimed at people who have some familiarity with high-resolution NMR and who wish to deepen their understanding of how NMR experiments actually ‘work’. This revised and updated edition takes the same approach as the highly-acclaimed first edition. The text concentrates on the description of commonly-used experiments and explains in detail the theory behind how such experiments work. The quantum mechanical tools needed to analyse pulse sequences are introduced set by step, but the approach is relatively informal